X-ray photoelectron spectroscopy (XPS) analyses of Fe(III)ΣFe were calibrated with nine single crystals of biotite of known Fe(III)ΣFe content. Peak shape parameters for the component Fe2+ and Fe3+ Fe 3p peaks were obtained ...
X-ray photoelectron spectroscopy (XPS) was used to determine Fe(III)ΣFe in individual biotite crystals in thin sections of ten metapelites and one syenite. The in situ XPS analyses of Fe(III)ΣFe in biotite crystals in the ...
Large single crystals of biotite and near-endmember phlogopite were reacted with aqueous solutions bearing 20 μM Cr(VI) and different concentrations of NaCl, LiCl, RbCl, CsCl, NaClO4, and Na2SO4. Solutions were maintained ...