FE AND NI IMPURITIES IN SYNTHETIC DIAMOND

dc.contributor.authorMeng Y.
dc.contributor.authorNewville M.
dc.contributor.authorSutton S.
dc.contributor.authorRakovan J.
dc.contributor.authorMao H.-K.
dc.date.accessioned2021-11-28T04:25:34Z
dc.date.available2021-11-28T04:25:34Z
dc.date.issued2003
dc.description.abstractUsing synchrotron X-ray fluorescence (XRF) microanalysis, including XRF tomography, and X-ray absorption near-edge structure (XANES) analyses, the distribution, and nature of incorporation of Fe and Ni impurities in as-grown diamond crystals, synthesized under high-pressure and high-temperature (HPHT) conditions, have been characterized. We find significantly different behavior for Fe and Ni as impurities in diamond. Nickel is dispersed and sector-zoned, with concentrations in {111} growth sectors at least 3 times those in {100} sectors, whereas Fe exists in the form of micro-aggregates or clusters with no observable sector correlation. Fe K-edge XANES shows that Fe is oxidized in diamond and has a valence of 2+. Comparison of XANES spectra from numerous standard compounds indicates that Fe is very likely bonded with oxygen as FeO.
dc.identifierhttps://www.elibrary.ru/item.asp?id=14175974
dc.identifier.citationAmerican Mineralogist, 2003, 88, 10, 1555-1559
dc.identifier.issn0003-004X
dc.identifier.urihttps://repository.geologyscience.ru/handle/123456789/32538
dc.subjectDiamond
dc.titleFE AND NI IMPURITIES IN SYNTHETIC DIAMOND
dc.typeСтатья

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